A novel low-temperature synthesis of nanosized NiZn ferrite

Seema Verma; S. D. Pradhan; Renu Pasricha; S. R. Sainkar; P. A. Joy

doi:10.1111/j.1551-2916.2005.00445.x

A novel low-temperature synthesis of nanosized NiZn ferrite

Seema Verma, S. D. Pradhan, Renu Pasricha, S. R. Sainkar, P. A. Joy

Core Technology Platforms

Research output: Contribution to journal › Article › peer-review

Abstract

Nanosized NiZn ferrite powder is synthesized by a low-temperature method, using a unique combination of citric acid and glycine. An appropriate molar ratio of both citric acid and glycine offers a low-temperature synthetic route by incorporating the complexation behavior of citric acid and the combustion nature of glycine. Thermal decomposition/controlled autocatalytic combustion of the composite gel occurs at a low temperature of around 175°C, with the evolution of a large amount of gases. Transmission electron microscopic studies showed that the average particle size of the ferrite obtained is ∼2.5 nm, with a narrow size distribution. Uniformly distributed fine-grained microstructure with low porosity is obtained for a sample sintered at 1000°C.

Original language	English (US)
Pages (from-to)	2597-2599
Number of pages	3
Journal	Journal of the American Ceramic Society
Volume	88
Issue number	9
DOIs	https://doi.org/10.1111/j.1551-2916.2005.00445.x
State	Published - Sep 2005

ASJC Scopus subject areas

Ceramics and Composites
Materials Chemistry

Access to Document

10.1111/j.1551-2916.2005.00445.x

Cite this

@article{7f8e4d4472964deb840080d6047b4e42,

title = "A novel low-temperature synthesis of nanosized NiZn ferrite",

abstract = "Nanosized NiZn ferrite powder is synthesized by a low-temperature method, using a unique combination of citric acid and glycine. An appropriate molar ratio of both citric acid and glycine offers a low-temperature synthetic route by incorporating the complexation behavior of citric acid and the combustion nature of glycine. Thermal decomposition/controlled autocatalytic combustion of the composite gel occurs at a low temperature of around 175°C, with the evolution of a large amount of gases. Transmission electron microscopic studies showed that the average particle size of the ferrite obtained is ∼2.5 nm, with a narrow size distribution. Uniformly distributed fine-grained microstructure with low porosity is obtained for a sample sintered at 1000°C.",

author = "Seema Verma and Pradhan, {S. D.} and Renu Pasricha and Sainkar, {S. R.} and Joy, {P. A.}",

year = "2005",

month = sep,

doi = "10.1111/j.1551-2916.2005.00445.x",

language = "English (US)",

volume = "88",

pages = "2597--2599",

journal = "Journal of the American Ceramic Society",

issn = "0002-7820",

publisher = "Wiley-Blackwell",

number = "9",

}

TY - JOUR

T1 - A novel low-temperature synthesis of nanosized NiZn ferrite

AU - Verma, Seema

AU - Pradhan, S. D.

AU - Pasricha, Renu

AU - Sainkar, S. R.

AU - Joy, P. A.

PY - 2005/9

Y1 - 2005/9

N2 - Nanosized NiZn ferrite powder is synthesized by a low-temperature method, using a unique combination of citric acid and glycine. An appropriate molar ratio of both citric acid and glycine offers a low-temperature synthetic route by incorporating the complexation behavior of citric acid and the combustion nature of glycine. Thermal decomposition/controlled autocatalytic combustion of the composite gel occurs at a low temperature of around 175°C, with the evolution of a large amount of gases. Transmission electron microscopic studies showed that the average particle size of the ferrite obtained is ∼2.5 nm, with a narrow size distribution. Uniformly distributed fine-grained microstructure with low porosity is obtained for a sample sintered at 1000°C.

AB - Nanosized NiZn ferrite powder is synthesized by a low-temperature method, using a unique combination of citric acid and glycine. An appropriate molar ratio of both citric acid and glycine offers a low-temperature synthetic route by incorporating the complexation behavior of citric acid and the combustion nature of glycine. Thermal decomposition/controlled autocatalytic combustion of the composite gel occurs at a low temperature of around 175°C, with the evolution of a large amount of gases. Transmission electron microscopic studies showed that the average particle size of the ferrite obtained is ∼2.5 nm, with a narrow size distribution. Uniformly distributed fine-grained microstructure with low porosity is obtained for a sample sintered at 1000°C.

UR - http://www.scopus.com/inward/record.url?scp=27644587056&partnerID=8YFLogxK

UR - http://www.scopus.com/inward/citedby.url?scp=27644587056&partnerID=8YFLogxK

U2 - 10.1111/j.1551-2916.2005.00445.x

DO - 10.1111/j.1551-2916.2005.00445.x

M3 - Article

AN - SCOPUS:27644587056

SN - 0002-7820

VL - 88

SP - 2597

EP - 2599

JO - Journal of the American Ceramic Society

JF - Journal of the American Ceramic Society

IS - 9

ER -

A novel low-temperature synthesis of nanosized NiZn ferrite

Abstract

ASJC Scopus subject areas

Access to Document

Other files and links

Fingerprint

Cite this