CHAPTER 2: The Methodology of Electrochemical in Situ NMR and MRI

Mingxue Tang; Riqiang Fu; Michaël Deschamps; K. Romanenko; A. Jerschow

doi:10.1039/9781839160097-00071

CHAPTER 2: The Methodology of Electrochemical in Situ NMR and MRI

Mingxue Tang, Riqiang Fu, Michaël Deschamps, K. Romanenko, A. Jerschow

Chemistry

Research output: Chapter in Book/Report/Conference proceeding › Chapter

Abstract

Non-destructive Nuclear Magnetic Resonance (NMR) plays a crucial role to unveil mechanisms of batteries under operation conditions. In situ NMR characterization offers intermediate information, which is very important for the performance of working devices, such as diffusion, kinetics, and dynamics that cannot be obtained by conventionalex situ approaches. This chapter introduces general considerations for performing in situ NMR experiments and summarizes designs of battery cells used for in situ NMR characterization. In addition, Magnetic Resonance Imaging (MRI) is a powerful method for visualization of materials with the aid of a magnetic field gradient to encode positions of nuclear spins. In situ MRI studies have contributed to an understanding of the fundamental phenomena that are associated with a battery's performance and failure mechanisms. Here we provide an overview of "electrochemical MRI"developments over the past two decades.

Original language	English (US)
Title of host publication	NMR and MRI of Electrochemical Energy Storage Materials and Devices
Editors	Yong Yang, Riqiang Fu, Hua Huo
Publisher	Royal Society of Chemistry
Pages	71-105
Number of pages	35
Edition	25
DOIs	https://doi.org/10.1039/9781839160097-00071
State	Published - 2021

Publication series

Name	New Developments in NMR
Number	25
Volume	2021-January
ISSN (Print)	2044-253X
ISSN (Electronic)	2044-2548

ASJC Scopus subject areas

Analytical Chemistry
Radiology Nuclear Medicine and imaging
Spectroscopy

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10.1039/9781839160097-00071

Cite this

Tang, M., Fu, R., Deschamps, M., Romanenko, K., & Jerschow, A. (2021). CHAPTER 2: The Methodology of Electrochemical in Situ NMR and MRI. In Y. Yang, R. Fu, & H. Huo (Eds.), NMR and MRI of Electrochemical Energy Storage Materials and Devices (25 ed., pp. 71-105). (New Developments in NMR; Vol. 2021-January, No. 25). Royal Society of Chemistry. https://doi.org/10.1039/9781839160097-00071

CHAPTER 2 : The Methodology of Electrochemical in Situ NMR and MRI. / Tang, Mingxue; Fu, Riqiang; Deschamps, Michaël; Romanenko, K.; Jerschow, A.

NMR and MRI of Electrochemical Energy Storage Materials and Devices. ed. / Yong Yang; Riqiang Fu; Hua Huo. 25. ed. Royal Society of Chemistry, 2021. p. 71-105 (New Developments in NMR; Vol. 2021-January, No. 25).

Research output: Chapter in Book/Report/Conference proceeding › Chapter

Tang, M, Fu, R, Deschamps, M, Romanenko, K & Jerschow, A 2021, CHAPTER 2: The Methodology of Electrochemical in Situ NMR and MRI. in Y Yang, R Fu & H Huo (eds), NMR and MRI of Electrochemical Energy Storage Materials and Devices. 25 edn, New Developments in NMR, no. 25, vol. 2021-January, Royal Society of Chemistry, pp. 71-105. https://doi.org/10.1039/9781839160097-00071

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note = "Funding Information: M.t. thanks the national natural science Foundation of China for support under grant no. 21974007, no. u1930401 and no. u1530402. r.F acknowledges support from the national high Magnetic Field lab (nhMFl), which is supported by the nsF Cooperative agreement DMr-1644779 and the state of Florida. M.D. acknowledges support from French network on electrochemical energy storage (rs2e - Fr 3459 Cnrs) and laboratory of excellence program store-ex (anr 10-laBx-0076). K. r. and a. J. thank professor philp w. Kuchel for valuable comments and manuscript edits, and acknowledge funding from us national science Foundation (CBet 1804723) and the australian research Council (Discovery project grant, Dp190100510). Publisher Copyright: {\textcopyright} The Royal Society of Chemistry 2021.",

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CHAPTER 2: The Methodology of Electrochemical in Situ NMR and MRI

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