Optimizing the Synthesis of Monodisperse Colloidal Spheres Using Holographic Particle Characterization

Christine Middleton; Mark D. Hannel; Andrew D. Hollingsworth; David J. Pine; David G. Grier

doi:10.1021/acs.langmuir.9b00012

Optimizing the Synthesis of Monodisperse Colloidal Spheres Using Holographic Particle Characterization

Christine Middleton, Mark D. Hannel, Andrew D. Hollingsworth, David J. Pine, David G. Grier

Chemical and Biomolecular Engineering

Research output: Contribution to journal › Article › peer-review

Abstract

Holographic particle characterization measures the sizes and compositions of individual colloidal particles dispersed in fluid media and rapidly amasses statistics on the distributions of these properties, even for complex heterogeneous dispersions. This information is useful for analyzing and optimizing protocols for synthesizing colloidal particles. We illustrate how holographic characterization can guide process design through a case study on a particularly versatile model system composed of an aqueous dispersion of micrometer-scale spheres synthesized from the organosilane monomer 3-(trimethoxysilyl)-propyl methacrylate (Figure Presented).

Original language	English (US)
Pages (from-to)	6602-6609
Number of pages	8
Journal	Langmuir
Volume	35
Issue number	20
DOIs	https://doi.org/10.1021/acs.langmuir.9b00012
State	Published - May 21 2019

ASJC Scopus subject areas

General Materials Science
Condensed Matter Physics
Surfaces and Interfaces
Spectroscopy
Electrochemistry

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10.1021/acs.langmuir.9b00012

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title = "Optimizing the Synthesis of Monodisperse Colloidal Spheres Using Holographic Particle Characterization",

abstract = "Holographic particle characterization measures the sizes and compositions of individual colloidal particles dispersed in fluid media and rapidly amasses statistics on the distributions of these properties, even for complex heterogeneous dispersions. This information is useful for analyzing and optimizing protocols for synthesizing colloidal particles. We illustrate how holographic characterization can guide process design through a case study on a particularly versatile model system composed of an aqueous dispersion of micrometer-scale spheres synthesized from the organosilane monomer 3-(trimethoxysilyl)-propyl methacrylate (Figure Presented).",

author = "Christine Middleton and Hannel, {Mark D.} and Hollingsworth, {Andrew D.} and Pine, {David J.} and Grier, {David G.}",

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AU - Pine, David J.

AU - Grier, David G.

PY - 2019/5/21

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AB - Holographic particle characterization measures the sizes and compositions of individual colloidal particles dispersed in fluid media and rapidly amasses statistics on the distributions of these properties, even for complex heterogeneous dispersions. This information is useful for analyzing and optimizing protocols for synthesizing colloidal particles. We illustrate how holographic characterization can guide process design through a case study on a particularly versatile model system composed of an aqueous dispersion of micrometer-scale spheres synthesized from the organosilane monomer 3-(trimethoxysilyl)-propyl methacrylate (Figure Presented).

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Optimizing the Synthesis of Monodisperse Colloidal Spheres Using Holographic Particle Characterization

Abstract

ASJC Scopus subject areas

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