Surface characterization of Ti and Y-TZP following non-thermal plasma exposure

Nelson R F A Silva; Paulo G. Coelho; Guilherme B. Valverde; Kurt Becker; Roland Ihrke; Antje Quade; Van P. Thompson

doi:10.1002/jbm.b.31887

Surface characterization of Ti and Y-TZP following non-thermal plasma exposure

Nelson R F A Silva, Paulo G. Coelho, Guilherme B. Valverde, Kurt Becker, Roland Ihrke, Antje Quade, Van P. Thompson

Research output: Contribution to journal › Article › peer-review

Abstract

Novel non-thermal plasma (NTP) technology has the potential to address the bonding issues of Y-TZP and Ti surfaces. This study aims to chemically characterize and evaluate the surface energy (SE) of Y-TZP and Ti surfaces after NTP application. Y-TZP and Ti discs were treated with a hand-held NTP device followed by SE evaluation. Spectra of Y-TZP 3d and Ti 2p regions, survey scans, and quantification of the elements were performed via X-ray photoelectron Spectroscopy (XPS) prior and after NTP. Separate Y-TZP and Ti discs were NTP treated for contact angle readings using (10-methacryloyloxydecyl dihydrogenphosphate) MDP primer. Significant augmentation of SE values was observed in all NTP treated groups. XPS detected a large increase in the O element fraction on both Y-TZP and Ti surfaces. Reduction of contact angle reading was obtained when the MDP primer was placed on NTP treated Y-TZP. Ti surface showed high SE before and after NTP application on Ti surfaces. NTP decreased C and increased O on both surfaces independently of application protocol. Wettability of MDP primer on Y-TZP was significantly increased after NTP. The high polarity obtained on Y-TZP and Ti surfaces after NTP applications appear promising to enhance bonds.

Original language	English (US)
Pages (from-to)	199-206
Number of pages	8
Journal	Journal of Biomedical Materials Research - Part B Applied Biomaterials
Volume	99 B
Issue number	1
DOIs	https://doi.org/10.1002/jbm.b.31887
State	Published - Oct 2011

Keywords

Y-TZP
adhesive
contact angle
non-thermal plasma
surface energy
titanium
wettability

ASJC Scopus subject areas

Biomaterials
Biomedical Engineering

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10.1002/jbm.b.31887

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title = "Surface characterization of Ti and Y-TZP following non-thermal plasma exposure",

abstract = "Novel non-thermal plasma (NTP) technology has the potential to address the bonding issues of Y-TZP and Ti surfaces. This study aims to chemically characterize and evaluate the surface energy (SE) of Y-TZP and Ti surfaces after NTP application. Y-TZP and Ti discs were treated with a hand-held NTP device followed by SE evaluation. Spectra of Y-TZP 3d and Ti 2p regions, survey scans, and quantification of the elements were performed via X-ray photoelectron Spectroscopy (XPS) prior and after NTP. Separate Y-TZP and Ti discs were NTP treated for contact angle readings using (10-methacryloyloxydecyl dihydrogenphosphate) MDP primer. Significant augmentation of SE values was observed in all NTP treated groups. XPS detected a large increase in the O element fraction on both Y-TZP and Ti surfaces. Reduction of contact angle reading was obtained when the MDP primer was placed on NTP treated Y-TZP. Ti surface showed high SE before and after NTP application on Ti surfaces. NTP decreased C and increased O on both surfaces independently of application protocol. Wettability of MDP primer on Y-TZP was significantly increased after NTP. The high polarity obtained on Y-TZP and Ti surfaces after NTP applications appear promising to enhance bonds.",

keywords = "Y-TZP, adhesive, contact angle, non-thermal plasma, surface energy, titanium, wettability",

author = "Silva, {Nelson R F A} and Coelho, {Paulo G.} and Valverde, {Guilherme B.} and Kurt Becker and Roland Ihrke and Antje Quade and Thompson, {Van P.}",

year = "2011",

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AU - Silva, Nelson R F A

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AU - Valverde, Guilherme B.

AU - Becker, Kurt

AU - Ihrke, Roland

AU - Quade, Antje

AU - Thompson, Van P.

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AB - Novel non-thermal plasma (NTP) technology has the potential to address the bonding issues of Y-TZP and Ti surfaces. This study aims to chemically characterize and evaluate the surface energy (SE) of Y-TZP and Ti surfaces after NTP application. Y-TZP and Ti discs were treated with a hand-held NTP device followed by SE evaluation. Spectra of Y-TZP 3d and Ti 2p regions, survey scans, and quantification of the elements were performed via X-ray photoelectron Spectroscopy (XPS) prior and after NTP. Separate Y-TZP and Ti discs were NTP treated for contact angle readings using (10-methacryloyloxydecyl dihydrogenphosphate) MDP primer. Significant augmentation of SE values was observed in all NTP treated groups. XPS detected a large increase in the O element fraction on both Y-TZP and Ti surfaces. Reduction of contact angle reading was obtained when the MDP primer was placed on NTP treated Y-TZP. Ti surface showed high SE before and after NTP application on Ti surfaces. NTP decreased C and increased O on both surfaces independently of application protocol. Wettability of MDP primer on Y-TZP was significantly increased after NTP. The high polarity obtained on Y-TZP and Ti surfaces after NTP applications appear promising to enhance bonds.

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Surface characterization of Ti and Y-TZP following non-thermal plasma exposure

Abstract

Keywords

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