X-ray and spectroscopic re-investigation of the 1:1 complex formed between urotropine and resorcinol

S. W. Ng, P. Naumov, A. R. Ibrahim, H. K. Fun, S. Chantrapromma, G. Wojciechowski, B. Brzezinski, J. V. Hanna

Research output: Contribution to journalArticle

Abstract

The 1:1 urotropine-resorcinol complex, which has been previously described in the non-centric C2cm space group, is redetermined in the centrosymmetric Cmcm space group. In the crystal structure, the urotropine moiety is linked to the resorcinol moiety by a single hydrogen bond [O···N = 2.769(4) Å]. The FT IR spectrum of the complex reflects the crystallographic features of the disordered structure.

Original languageEnglish (US)
Pages (from-to)89-95
Number of pages7
JournalJournal of Molecular Structure
Volume609
Issue number1-3
DOIs
StatePublished - May 30 2002

Keywords

  • C NMR
  • Crystal structure
  • FT IR spectroscopy
  • H NMR
  • Intermolecular hydrogen bond
  • Solid-state C NMR
  • Urotropine

ASJC Scopus subject areas

  • Analytical Chemistry
  • Spectroscopy
  • Organic Chemistry
  • Inorganic Chemistry

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  • Cite this

    Ng, S. W., Naumov, P., Ibrahim, A. R., Fun, H. K., Chantrapromma, S., Wojciechowski, G., Brzezinski, B., & Hanna, J. V. (2002). X-ray and spectroscopic re-investigation of the 1:1 complex formed between urotropine and resorcinol. Journal of Molecular Structure, 609(1-3), 89-95. https://doi.org/10.1016/S0022-2860(01)00945-0